In this chapter, a solid state Nuclear Magnetic Resonance (ss-NMR) Study of sixteenth century book is reported. Cross polarization Magic Angle Spinning Nuclear Magnetic Resonance (13C(1H) CP MAS NMR) spectra of paper samples collected from the book, allowed us to obtain information on its state of conservation. The physico-chemical characterization of two parchment samples collected from the cover book was performed trough the evaluation of the changes in line width and intensity of signals in the spectra.
Spinella, A., Capitani, D., Bastone, S., Di Stefano, V., Caponetti E (2013). Solid state NMR to characterize paper and parchment samples from a Sixteenth century book. In E. Varella (a cura di), Conservation Science for the Cultural Heritage. Applications of Instrumental Analysis (pp. 208-217). Thessaloniki : Springer.
Solid state NMR to characterize paper and parchment samples from a Sixteenth century book
SPINELLA, Alberto;BASTONE, Stella;CAPONETTI, Eugenio
2013-01-01
Abstract
In this chapter, a solid state Nuclear Magnetic Resonance (ss-NMR) Study of sixteenth century book is reported. Cross polarization Magic Angle Spinning Nuclear Magnetic Resonance (13C(1H) CP MAS NMR) spectra of paper samples collected from the book, allowed us to obtain information on its state of conservation. The physico-chemical characterization of two parchment samples collected from the cover book was performed trough the evaluation of the changes in line width and intensity of signals in the spectra.
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